Abstract
A new methodology to study the precipitation crystallography of dispersoids in an Al matrix is proposed. By combining high angle annular dark field tomography and electron diffraction studies, the three-dimensional morphology, orientation relationship (OR) with Al matrix and habit planes of the dispersoids can be achieved simultaneously. This approach has been applied to investigate the -Al(Mn,Fe)Si dispersoids precipitated in an AA3xxx alloy. Most dispersoids have a plate-shaped morphology after low-temperature homogenization at 450
C. The largest proportion of the dispersoids follows the previously described OR with the Al matrix
. Two plate-shaped dispersoids have been studied in detail. The dispersoid following the commonly observed orientation had habit planes
. The dispersoid not following the commonly observed OR had habit planes
, with (OR)
,
.
Notes
Supplemental data for this article can be accessed here http://dx.doi.org/10.1080/14786435.2015.1006294.