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Part A: Materials Science

Bubble-loop complexes induced by helium irradiation and effect of pre-irradiation and post-irradiation of hydrogen in reduced-activation ferritic/martensitic steel

, , , , , , & show all
Pages 2495-2511 | Received 27 Dec 2017, Accepted 11 Jun 2018, Published online: 03 Jul 2018
 

ABSTRACT

In the present work, the synergistic effect of high concentration hydrogen and helium on the dislocation loops and bubbles as well as their correlations in reduced-activation ferritic/martensitic (RAFM) steels is investigated. Such an effect was transmuted from 14 MeV neutron irradiation and has been one of the most challenging issues for RAFM steels for future fusion reactors. After low dose (0.18 dpa) high concentration (5000 appm) single-ion helium irradiation at 723 K, very large dislocation loops were observed, and the majority of bubbles were inside dislocation loops, forming bubble-loop complexes. These bubble-loop complexes defects were also present in hydrogen/helium and helium/hydrogen sequential-ion irradiated steels. Pre-irradiated hydrogen ion effectively inhibited the later growth of loops induced by helium post-irradiation, and the higher the ratio of hydrogen to helium fluence, the greater the effect of inhibition. At high fluence of hydrogen pre-irradiation, the structure of bubble-loop complexes disappeared. On the other hand, hydrogen post-irradiation promoted the growth of loops induced by helium pre-irradiation, and the higher the ratio of hydrogen to helium fluence, the greater the effect of promotion. The mechanisms for hydrogen/helium synergistic effects are discussed.

Acknowledgements

The authors would like to thank the Center for Electron Microscopy at Wuhan University, China.

Disclosure statement

No potential conflict of interest was reported by the authors.

Additional information

Funding

Financial support from the National Natural Science Foundation of China [11775162], [U1532134] and the International Science & Technology Cooperation Program of China [2015DFR60370] are gratefully acknowledged.

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