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Fabrications and Characterization of Organic Materials

Heating Temperature Effect on the Magnetic Property of α-Fe Nanoparticle

, , &
Pages 69/[459]-75/[465] | Published online: 22 Sep 2010
 

Abstract

The effect of heating temperature on the magnetic property of α-Fe nanoparticle produced by thermal decomposition method has been investigated. The Fe2+-oleate2 ligand complex was annealed at 400°C in pyrex tube under 10−2 torr for 2 hrs, and then reduced at a different temperatures under Ar + 4% H2 mixture gas atmosphere. The magnetic property of α-Fe nanocrystallite was affected with the different heating temperatures. The structure and properties of prepared α-Fe nanoparticle was characterized by TGA, XRD, TEM, and VSM.

Acknowledgments

Young Chul Han would like to thank to the financial support by Brain Korea 21 project in 2006.

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