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Molecular Crystals and Liquid Crystals Volume 493, 2008 - Issue 1
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Liquid Crystals

Synthesis and Mesomorphic Properties of Some Chiral Fluorinated Benzoates

Yongmin Guo Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou (Soochow) University, Suzhou, Jiangsu, China
,
Baozong Li Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou (Soochow) University, Suzhou, Jiangsu, China
,
Yonggang Yang Key Laboratory of Organic Synthesis of Jiangsu Province, College of Chemistry and Chemical Engineering, Suzhou (Soochow) University, Suzhou, Jiangsu, ChinaCorrespondence[email protected]
&
Jianxun Wen Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai, China
Pages 57-64 | Published online: 01 Aug 2011
 
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Abstract

One series of chiral fluorinated benzoates have been synthesized. These compounds were characterized by IR, 1H NMR, 19F NMR, MS, and elemental analysis. Their phase transition behavior was investigated by DSC and polarizing optical microscopy. Generally, they show an enantiotropic SmA phase. The effect of lateral and terminal fluoro-substitution was studied in this series.

ACKNOWLEDGMENTS

This work was partially supported by Jiangsu Provincial Key Laboratory of Organic Chemistry Foundation and Natural Science Foundation of Jiansu Province (No. BK2007047).

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