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LOW-DIMENSIONAL SOLIDS AND MOLECULAR CRYSTALS

Synthesis and Crystal Structure Characterization of (E)-Methyl 2-(Methoxyimino)-2-(2-((3-(6-(Trifluoromethyl) Pyridin-3-yl) Phenoxy) Methyl) Phenyl) Acetate

, , , &
Pages 264-271 | Published online: 26 Feb 2015
 

Abstract

The title compound, (E)-methyl 2-(methoxyimino)-2-(2-((3-(6-(trifluoromethyl)pyridin-3-yl) phenoxy) methyl) phenyl) acetate was synthesized and characterized by 1H and 13C NMR, IR, and MS spectroscopy. Its molecular structure was investigated by X-ray crystallography. The crystal structure analysis revealed that the two independent molecules interact via C‒H···O to form a dimer, which is further connected by weak interaction with another dimer to constitute a four molecular crystal packing. At the same time, two molecules are linked by weak intermolecular C13-O3 and O3-H15 interactions to constitute a ring involving six atoms (C13/C12/C14/C15/H15/O3), which are not in the same plane. Compound (5) crystallizes in a monoclinic system, space group P121/c1, a = 7.2024(4) Å, b = 8.4592(6) Å, c = 35.389(2) Å.

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