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Molecular Crystals and Liquid Crystals Volume 675, 2018 - Issue 1
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Articles

Crystal Structure and Fluorescent Properties of Cd(II) Complexes Based on Acylhydrazone ligands

Zhen-Ni GouCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Shun-Sheng ZhaoCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China; ;Key Laboratory of Coal Resources Exploration and Comprehensive Utilization, Ministry of Land and Resources, Xi’an710021, P. R. ChinaCorrespondence[email protected]
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Pan ZhangCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Xing YuCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Jing-Jing LiuCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Zai-Wen YangCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Zheng YangCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Xiao-Dan JiaCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Xin-Yue WangCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China;
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Xiang-Rong LiuCollege of Chemistry and Chemical Engineering, Xi’an University of Science and Technology, Xi’an710054, P. R. China; ;Key Laboratory of Coal Resources Exploration and Comprehensive Utilization, Ministry of Land and Resources, Xi’an710021, P. R. China
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Pages 75-84 | Published online: 27 Jun 2019
 
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Abstract

8-Hydroxyquinoline-2-carbaldehyde-(4'-hydroxyphenylacetyl) hydrazine (HL) and Its complexes ([Cd(L)2·CH3CH2OH·8H2O] (1), [Cd(HL)2][CdCl4]·3CH3CH2OH·2H2O] (2) were synthesized from 8-hydroxyquinoline-2-carbaldehyde and 2-(4-hydroxyphenyl)acetohydrazide as starting materials. The structures of two complexes have been characterized by single crystal X-ray diffraction, elemental analysis and Fourier transform infrared spectroscopy. X-ray diffraction analysis shows that both of complexes 1 and 2 crystallized in triclinic space group Pī. Also, the fluorescence properties of complex were studied by UV-Vis absorption by fluorescence spectroscopy, and the thermal stability was investigated by thermogravimetric analysis.

Acknowledgment

This research was supported by the National Natural Science Foundation of China (NOs. 21103135, 21073139, 21301139 and 21373158), Shaanxi innovative Talent Promotion Project (NO. 2017KJXX-55) and Natural Science Basic Research Plan in Shaanxi Province of China (NOs. 2016JM2011 and 2018JQ2061).

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