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Molecular Crystals and Liquid Crystals Volume 726, 2021 - Issue 1
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Low-Dimensional Solids and Molecular Crystals

A novel crystal of kanamycin disulfate: Preparation, structure and hygroscopicity

Zhao-Zhen LiuNMPA Key Laboratory for Research and Evaluation of Generic Drugs, Beijing Key Laboratory of Analysis and Evaluation on Chinese Medicine, Beijing Institute for Drug Control, Beijing, ChinaView further author information
,
Bao-Quan CheNMPA Key Laboratory for Research and Evaluation of Generic Drugs, Beijing Key Laboratory of Analysis and Evaluation on Chinese Medicine, Beijing Institute for Drug Control, Beijing, ChinaView further author information
,
Jun-Qiu WangNMPA Key Laboratory for Research and Evaluation of Generic Drugs, Beijing Key Laboratory of Analysis and Evaluation on Chinese Medicine, Beijing Institute for Drug Control, Beijing, ChinaCorrespondence[email protected] [email protected]
View further author information
&
Wen-Dong LiNMPA Key Laboratory for Research and Evaluation of Generic Drugs, Beijing Key Laboratory of Analysis and Evaluation on Chinese Medicine, Beijing Institute for Drug Control, Beijing, ChinaCorrespondence[email protected] [email protected]
View further author information
Pages 51-55 | Published online: 25 Jun 2021
 
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Abstract

A new kanamycin disulfate compound with chair structure has been successfully synthesized by volatilization method. The structure of the compound kanamycin disulfate was determined by single-crystal and powder X-ray crystallography. The decline of hygroscopicity made the kanamycin easier to save.

Acknowledgments

We thank the NMPA Key Laboratory for Research and Evaluation of Generic Drugs.

Disclosure statement

There are no conflicts to declare.

Additional information

Funding

This work is financially supported by the Chinese Pharmacopeia Commission (grant number 2014322).

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