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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 37, 2007 - Issue 4
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Original Articles

Synthesis and Characterization of Some CoIII and CrIII Complexes Containing Diazine Ligands

A. Mobinikhaled Department of Chemistry, University of Arak, Arak, IranCorrespondence[email protected]
,
N. Foroughifar Department of Chemistry, University of Arak, Arak, Iran
&
M. Zendehdel Department of Chemistry, University of Arak, Arak, Iran
Pages 225-228 | Received 31 Dec 2006, Accepted 13 Feb 2007, Published online: 09 May 2007
 
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Preparation and characterization of a number of CoIII and CrIII complexes containing one heterocyclic ligand was reported. The complexes [(NH3)5ML](ClO4)3 (M˭Co, Cr, L=phthalazine, 1‐methylphthalazine, pyridazine, 3‐methylpyridazine) were prepared by reaction of triflato complex [(NH3)5MOSO2CF3] (CF3SO3)2 with the appropriate ligand in sulfolane. These complexes were recrystallized in warm water by addition of NaClO4 and characterized by 1H and 13C NMR spectroscopy and elemental analysis. NOE and DESERT experiments were carried out in order to characterize the position of coordination.

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