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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 37, 2007 - Issue 8
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Original Articles

Synthesis, Crystal Structure and Properties of the Enantiotopic Complex Constructed From Chiral Ligand H2bpb, [Co(H2bpb)2(NCS)2(CH3OH)2] (H2bpb=1,2‐Bis(3‐pyridylcarboxamide)benzene)

Ping Zhang Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. China
,
Ben‐Lai Wu Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. China
,
Yun‐Yin Niu Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. China
,
Hong‐Yun Zhang Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. ChinaCorrespondence[email protected]
,
Cao‐Yuan Niu Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. China
&
Hong‐Wei Hou Department of Chemistry, Zhengzhou University, Zhengzhou, P. R. China
Pages 577-582 | Received 07 Feb 2007, Accepted 12 Apr 2007, Published online: 02 Oct 2007
 
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A six‐coordinating cobalt () complex, [Co(H2bpb)2(NCS)2(CH3OH)2], where H2bpb is 1,2‐bis(3‐pyridylcarboxamide)benzene, was prepared and characterized by IR spectrum and thermal analysis, its crystal structure was determined X‐ray analysis. It crystallizes in the triclinic system with space group P‐1 with a=8.7005(9) Å, b=9.6114(10) Å, c=13.767(2) Å, α= 101.393(2)o, β=93.185(2)o, γ=114.5180(10)o, V=1014.5(2) Å, Z=1. Fluorescent and thermal properties of the complex were also investigated.

We gratefully acknowledge financial support from the National Natural Science Foundation of China (20671083) and the Science and Technology Foundation of Henan Province (0524270061).

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