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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 37, 2007 - Issue 8
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Original Articles

Synthesis, Crystal Structure and Electrochemistry of Ferrocene‐Containing Diketoimines

Mei‐Jun Zhu College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China
,
Jing Sun College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China
,
Yao‐Cheng Shi College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, China
&
Chao‐Guo Yan College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou, ChinaCorrespondence[email protected]
Pages 633-637 | Received 22 Mar 2007, Accepted 10 May 2007, Published online: 01 Oct 2007
 
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Acetoacetylferrocene reacted with benzidine and 4,4′‐diaminodiphenylmethane in absolute ethanol to give the diketoimines 2a–b in high yields. Determined by X‐ray structure analysis, 2a crystallized in monoclinic crystal system—space group P21/c with cell parameters: a=10.8595(2), b=12.4095(2), c=12.2021(2) Å, β=97.6390(10), Z=2, V=1631.10(5) Å3. The unit cell contains two independent molecules to form helical crystal structure stabilized by hydrogen bond interactions with helical angle is 39.3°.

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