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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 37, 2007 - Issue 9
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Original Articles

42‐ and 46‐Membered Phosphorus‐Based Macrocycles

Vadapalli Chandrasekhar Department of Chemistry, Indian Institute of Technology, Kanpur, IndiaCorrespondence[email protected]
,
Gurusamy Thangavelu Senthil Andavan Department of Chemistry, Indian Institute of Technology, Kanpur, India
,
Ramachandran Azhakar Department of Chemistry, Indian Institute of Technology, Kanpur, India
&
Balasubramanian Murugesa Pandian Department of Chemistry, Indian Institute of Technology, Kanpur, India
Pages 725-728 | Received 15 Nov 2006, Accepted 09 May 2007, Published online: 06 Nov 2007
 
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Abstract

42‐ and 46‐Membered phosphorus‐based macrocycles were obtained in a [2+2] condensation of PhP(O)[N(Me)NH2]2 with dialdehydes. These macrocycles were isolated in a pure form after preparative thin layer chromatography and were characterized by multinuclear NMR and mass spectroscopy. The FAB mass spectra of these macrocycles revealed parent ion (M+1) peaks in good intensity.

Acknowledgments

Dedicated to Prof. Dr. H.W. Roesky in recognition of his outstanding contributions to Inorganic and Organometallic Chemistry.

We thank the Department of Science and Technology, India and the Council of Scientific and Industrial Research, India for financial support. R. A. thanks IIT Kanpur for financial assistance. B. M. P. thanks the Council of Scientific and Industrial Research for a Senior Research Fellowship.

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