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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 37, 2007 - Issue 10
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Original Articles

Supercritical Carbon Dioxide‐Soluble Fluorus vic‐Dioxime Ligands and their NiII Complexes: Synthesis, Characterization and Solubility Properties

B. Guzel Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, TurkeyCorrespondence[email protected]
,
G. Avşar Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, Turkey
&
H. F. Çınkır Faculty of Sciences and Letters, Chemistry Department, Çukurova University, Adana, Turkey
Pages 801-804 | Received 12 Jul 2007, Accepted 03 Oct 2007, Published online: 29 Nov 2007
 
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New supercritical carbon dioxide s oluble ligands, N,N′‐bis(4‐trifluoromethyl phenylamino)glyoxime, N,N′‐bis(3‐trifluoromethylphenylamino)glyoxime, N,N′‐bis(3,5‐ditrifluoromethyl phenylamino)glyoxime and their NiII complexes have been prepared and characterized by spectroscopic methods and elemental analysis. The solubility of the synthesized ligands and their NiII complexes were measured at 343.15 K and 172.4 bar in supercritical carbon dioxide.

We are grateful to Çukurova University Research Foundation for financial support (FEF2003BAP5).

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