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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 40, 2010 - Issue 6
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Original Articles

Meso-tetra[(p-alkoxyl-m-ethyloxy)phenyl]porphyrins and their Transition Metal Complexes: Synthesis and Characterization

Miao Yu State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun, Jilin, P. R. China; College of Chemistry, Jilin University, Changchun, Jilin, P. R. China
,
Yu J. Zhang College of Chemistry, Jilin University, Changchun, Jilin, P. R. China
,
Jian H. Shi College of Chemistry, Jilin University, Changchun, Jilin, P. R. China
,
Guo F. Liu College of Chemistry, Jilin University, Changchun, Jilin, P. R. China
&
Hong J. Zhang State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun, Jilin, P. R. China
Pages 404-409 | Received 07 Sep 2009, Accepted 07 May 2010, Published online: 13 Jul 2010
 
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Abstract

Three meso-tetra[( p -alkoxyl- m -ethyloxy)phenyl]porphyrins and their transition metal (Zn, Cu, Ni, Co, Mn) complexes were synthesized. The molecular structures were confirmed by means of 1H NMR, UV-Vis, IR, elemental analyses, etc., which indicate the valence state of Mn atom in the compound is +3 and Ni, Cu, Zn, Co atom is +2. Optical properties were discussed by fluorescence spectrum. The quantum yields of the complexes are much lower than the corresponding ligands.

The authors are grateful to the financial support of the National Natural Science Foundation of China (No. 20801022).

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