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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 43, 2013 - Issue 9
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Original Articles

Synthesis, Characterization, and Structure of Ruthenium Complex Ru(dppe)2C2O4 (dppe = Ph2P(CH2)2PPh2)

Yi-Feng Zhou College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
,
Li-Hong Huang College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
,
Xiao-Hong Chen State Key Laboratory of Chemical Engineering, Beijing University of Chemical Technology, Beijing, P. R. China
,
Ji-Dong Lou College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
&
Xiu Lian Lu College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
Pages 1228-1230 | Received 03 Mar 2011, Accepted 29 Jul 2011, Published online: 14 May 2013
 
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Abstract

The title complex Ru(dppe)2C2O4 (dppe = Ph2P(CH2)2PPh2) was synthesized and determined by IR, NMR, elemental analysis, and X-ray crystallographic analysis. The structure shows Ru atom was coordinated with four phosphorus atoms of two dppe ligands and two oxygen atoms of oxalate ligand in a distorted octahedral geometry.

Acknowledgments

The authors thank the project of SRF for ROCS (000049), SEM and Ministry of Personnel (01017-080002), the State Key Laboratory of Chemical Resource Engineering, and Qianjiang Project of Zhejiang Province (01002-123-080050) for financial support.

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