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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 42, 2012 - Issue 7
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Original Articles

Synthesis and Structure of a Supramolecular Coordination Polymer [ZnI2L(CH3OH)(H2O)2]n (L = N-(3- (isonicotinamido) phenyl) isonicotinamide) With 1D Chain Structure

Zun-Zhe Shu College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China; College of Life Science, Tarim University, Alar, Xinjiang, P. R. China; Key Laboratory of Biological Resource Protection and Utilization of Tarim Basin, Xinjiang Production & Construction Group, Xinjiang, Alaer, Xinjiang, P. R. China
,
Ting Cao College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Hong-Mei Wang College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Xiao-Ling Guo College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Ming-Wen Yin College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Qi-Kun Han College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
,
Bao-Ding Li College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
&
Yun-Yin Niu College of Chemistry and Molecular Engineering, Zhengzhou University, Zhengzhou, P. R. China
 show all
Pages 999-1002 | Received 28 Aug 2011, Accepted 03 Jan 2012, Published online: 06 Aug 2012
 
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Abstract

Reaction of a ZnI2 solution in CH3OH/H2O with a solution of L in DMF gave rise to a novel 3D supramolecular compound [ZnI2L(CH3OH)(H2O)2]n based on 1D wavy chain. The crystal structural analysis indicated that the complex crystallized in a monoclinic space group C2/c, a = 29.381(6), b = 13.021(3), c = 13.959(3), β = 102.48(3), V = 5214.0(18) Å3, Z = 8. The complex possessed a 3-D supramolecular framework formed by intermolecular hydrogen bonding among 1D wavy chains.

Acknowledgments

The authors acknowledge the NSFC (Nos.21171148, J0830412, J1103309).

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