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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 43, 2013 - Issue 10
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Original Articles

An Improved Procedure for Oxidative Cleavage of Oximes to the Corresponding Carbonyl Compounds With Chromic Acid Supported on Kieselguhr Under Viscous Conditions

Fang Lin College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
,
Jianan Lin College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
,
Wenjin Zheng College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
,
Xiu Lian Lu College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China
&
Ji-Dong Lou College of Life Sciences, China Jiliang University, Hangzhou, Zhejiang, P. R. China; Sirnaomics, Inc., Gaithersburg, MD, USA
Pages 1518-1520 | Received 04 Dec 2011, Accepted 29 Dec 2012, Published online: 25 Aug 2013
 
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Abstract

An improved and efficient oxidative cleavage of oximes to the corresponding carbonyl compounds with chromic acid supported on kieselguhr reagent at room temperature under viscous conditions in the yield between 82% and 96% is described. The present procedure can overcome the problems that existed in the common solvent-free reactions as for the difficulty for the solid molecular collision to react.

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