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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 45, 2015 - Issue 6
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Original Articles

Hydrothermal In Situ Ligand Synthesis to Fabricate a New Heterometallic Cu(II)-Sr(II) Coordination Polymer: Synthesis, Structure, and Thermal Analysis

Yuan-Yuan HuangKey Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, P. R. China;Graduate School, Chinese Academy of Sciences, Beijing, P. R. China
,
Xin ZhangKey Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, P. R. China
,
Ming-Ling SunKey Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, P. R. China
&
Yuan-Gen YaoKey Laboratory of Coal to Ethylene Glycol and Its Related Technology, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, P. R. ChinaCorrespondence[email protected]
Pages 799-803 | Received 21 Aug 2013, Accepted 08 Sep 2013, Published online: 14 Nov 2014
 
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Abstract

A new heterometallic coordination polymer, [Cu2Sr(ipO)2(H2O)3]n·2n(H2O) (1 H3ipO = 2-hydroxyisophthalate), has been successfully synthesized and characterized. Single-crystal X-ray diffraction analysis reveals that compound 1 features a 2D layer structure based on butterfly-like [Cu2(ipO)2]2− metallo-ligand subunits, and can be simplified into a rare (3,6)-connected kgd topological network. Through intermolecular hydrogen bonds, this 2D sheet extends into a 3D supramolecular framework. In addition, thermal stability of this compound was also investigated.

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