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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 45, 2015 - Issue 7
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Original Articles

Syntheses, Characterization, and X-Ray Crystal Structures of Two New Crystals MgCl2·2H2O·2C2H4(OH)2 and MgCl2·6H2O·C2H4(OH)2

Zhen-Hua CuiKey Laboratory of Salt Lake Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining, P. R. China;University of Chinese Academy of Sciences, Beijing, P. R. China
,
Jin-He SunKey Laboratory of Salt Lake Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining, P. R. China
,
Yong-Zhong JiaKey Laboratory of Salt Lake Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining, P. R. ChinaCorrespondence[email protected]
,
Yan-Mei ChenKey Laboratory of Salt Lake Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining, P. R. China
&
Xiao-Ping JiangChemistry and Life Science College, Qinghai University for Nationality, Xining, P. R. China
Pages 1004-1010 | Received 17 Aug 2013, Accepted 02 Nov 2013, Published online: 09 Mar 2015
 
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Abstract

Two new crystals MgCl2·2H2O·2C2H4(OH)2 (1) and MgCl2·6H2O·C2H4(OH)2 (2) assembled by MgCl2·6H2O and C2H4(OH)2 have been synthesized. Structures of 1 and 2 have been determined by single-crystal X-ray diffraction analyses and elemental analyses, IR, Raman spectra, powder X-ray diffraction and TGA. The complex 1 is triclinic, space group P1 with a = 5.697(4) Å, b = 7.404(5) Å, c = 7.528(5) Å, β = 70.426(11)°, V = 268.3(3) Å3. Complex 2 is monoclinic, space group C2/c with a = 12.175(9) Å, b = 7.077(5) Å, c = 14.781(10) Å, β = 103.880(12)°, V = 1236.4(15) Å3.

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