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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 45, 2015 - Issue 8
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Original Articles

Synthesis and Characterization of AgSCN Micro/Nanostructures by Sonochemical Method

F. SoofivandInstitute of Nano Science and Nano Technology, University of Kashan, Kashan, I. R. Iran
,
M. Salavati-NiasariInstitute of Nano Science and Nano Technology, University of Kashan, Kashan, I. R. Iran;Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, I. R. IranCorrespondence[email protected]
,
F. MohandesDepartment of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, I. R. Iran
,
K. SaberyanFuel Cycle Research School, NSTRI, Tehran, I. R. Iran
&
Armen AvanesDepartment of Chemistry, Faculty of Science, University of Maragheh, Maragheh, I. R. Iran
Pages 1191-1198 | Received 24 Aug 2013, Accepted 10 Oct 2013, Published online: 26 Mar 2015
 
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Abstract

Silver (I) salicylate complex marked as [Ag(HSal)] was prepared, characterized, and applied to fabricate AgSCN micro/nanostructures. The [Ag(HSal)] complex was synthesized by silver nitrate and sodium salicylate via a simple precipitation route. To obtain AgSCN micro/nanostructures, the [Ag(HSal)] complex and KSCN were mixed with molar ratio of 1:1 in the presence of ultrasound irradiation. Besides, the effect of sonication time and surfactant on the morphology and particle size of the products was investigated. In this work, polyvinyl pyrrolidone was used as surfactant to prepare star-like and flower-like AgSCN microstructures. The products were analyzed by FT-IR, XRD, EDS, SEM, and TEM.

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