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Energy Sources, Part A: Recovery, Utilization, and Environmental Effects Volume 32, 2010 - Issue 6
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Original Articles

Solid Superacid-catalyzed Hydroconversion of Demineralized Shengli Coal Liquefaction Residue under Microwave Irradiation

Y.-B. Wei Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
Z.-M. Zong Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
R.-L. Xie Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
Y.-L. Peng Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
J. Mou Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
Y.-M. Ma Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
X. Zhou Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
Y. Huang Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
,
L. Wu Hubei Coal Conversion and New Carbon Materials Laboratory, Wuhan University of Science and Technology, Wuhan, Hubei, China
&
X.-Y. Wei Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China; Hubei Coal Conversion and New Carbon Materials Laboratory, Wuhan University of Science and Technology, Wuhan, Hubei, China
 show all
Pages 551-558 | Received 27 Sep 2008, Accepted 16 Oct 2008, Published online: 06 Jan 2010
 
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Abstract

Shengli coal liquefaction residue was demineralized; the demineralized Shengli coal liquefaction residue (DMSCLR) was then subject to non-catalytic and SO4 2−/ZrO2- or SO4 2−/TiO2-catalyzed hydroconversion in methanol under microwave irradiation. The results show that both, SO4 2−/ZrO2 and SO4 2−/TiO2, significantly catalyzed DMSCLR hydroconversion. The MESs of hydrogenated DMSCLR were analyzed with gas chromatography/mass spectrometer. The MESs and methanol-inextractable fractions of hydrogenated DMSCLR were characterized with Fourier transform infrared spectrometer.

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