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Energy Sources, Part A: Recovery, Utilization, and Environmental Effects Volume 32, 2010 - Issue 13
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Original Articles

The Microwave-assisted Hydrogenation of 9,10-Diphenylanthracene over Pd/C

Y. M. Ma Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China; Department of Chemical Engineering, Xinjiang Polytechnical College, Urumchi, Xinjiang, China
,
X. Zhou Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China; Department of Chemical Engineering, Xinjiang Polytechnical College, Urumchi, Xinjiang, China
,
X. Y. Wei Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China; Hubei Coal Conversion and New Carbon Materials Laboratory, Wuhan University of Science and Technology, Wuhan, Hubei, China
&
Z. M. Zong Key Laboratory of Coal Processing and Efficient Utilization (Ministry of Education), China University of Mining and Technology, Xuzhou, Jiangsu, China
Pages 1201-1206 | Received 03 Nov 2008, Accepted 04 Dec 2008, Published online: 23 Apr 2010
 
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Abstract

Palladium/activated carbon (Pd/C) catalyzed hydrogenation of 9,10-diphenylanthracene (DPA), used as a coal-related model compound, was investigated under microwave irradiation. The effects of reaction temperature, pressure, and time on DPA yield were studied. The results show that DPA hydrogenation proceeds at much lower temperatures and hydrogen pressure under microwave irradiation than those by conventional heating and Pd/C mainly promote ipso hydrogenation of DPA. The related mechanism was discussed.

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