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Original Articles

An expedient synthesis of methyl vinyl sulfide from dimethyl disulfide and acetylene

, , , , , , & show all
Pages 395-399 | Received 20 Sep 2004, Accepted 29 Sep 2004, Published online: 21 Aug 2006
 

Abstract

Dimethyl disulfide reacts with acetylene under atmospheric pressure in basic reductive systems MOH (M=Na, K)–N2H4 · H2O–N-methylpyrrolidone and Na2S · 9H2O–N2H4 · H2O–N-methylpyrrolidone to form methyl vinyl sulfide in up to 79% yield.

Acknowledgment

Financial support from the Ministry of Industry, Science and Technologies of the Russian Federation (grant No. NSH-2241.2003.3) is gratefully acknowledged.

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