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Journal of Sulfur Chemistry Volume 37, 2016 - Issue 2
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Original Articles

Reaction of dithiocarbamates with 2-[bis(methylthio)-methylene]malononitrile: unexpected formation of 4-imino-6-(methylthio)-3-substituted-3,4-dihydro-2H-1,3-thiazine-2-thionesFootnote

Tamer El MalahDepartment of Photochemistry, National Research Centre, Dokki, Egypt
,
Ashraf A. AlyDepartment of Chemistry, Faculty of Science, El-Minia University, El-Minia, EgyptCorrespondence[email protected]
,
Stefan BräseInstitute of Organic Chemistry, Karlsruhe Institute of Technology, Karlsruhe, Germany
,
N. A. A. ElkanziChemistry Department, Faculty of Science, Aswan University, Aswan, Egypt
&
Alan B. BrownChemistry Department, Florida Institute of Technology, Melbourne, FL, USA
Pages 222-228 | Received 11 Oct 2015, Accepted 13 Nov 2015, Published online: 20 Jan 2016
 
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Abstract

1,3-Thiazine-2-thione derivatives were obtained from the reaction between dithiocarbamates and 2-[bis(methylthio)-methylene]malononitrile. Evidence for the structure of the obtained products was obtained by IR, mass, and NMR spectra and elemental analysis. The reaction mechanism is also discussed.

GRAPHICAL ABSTRACT

Notes

* Dedicated to Professor Henning Hopf on the occasion of his 75th birthday.

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