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Research Article

A non-probabilistic convex modelling framework for uncertainty quantification of laser powder bed fusion fabricated structures based on limited data

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Article: e2324429 | Received 01 Sep 2023, Accepted 19 Feb 2024, Published online: 06 Mar 2024

ABSTRACT

Laser powder bed fusion (LPBF) is increasingly prominent in essential fields such as aerospace. However, due to the characteristics of the manufacturing process and the high test cost, the performance of fabricated structures is inherently uncertain, leading to a challenging characterisation of their performance. This paper proposes a non-probabilistic convex modelling framework involving confirming uncertainties, processing data, and establishing a non-probabilistic convex model, to quantitatively describe the uncertainties concerning the physical properties of structures fabricated by LPBF. Firstly, the non-probabilistic convex modelling framework is proposed and an efficient uncertainty quantification method is developed utilising the non-probabilistic convex model. Then, criteria are set up for evaluating the performance of the developed method, and computational efficiency and accuracy are illustrated via benchmark numerical examples. Last but not least, two types of representative structures, solid and lattice structures, are fabricated via the LPBF method. The physical properties are tested through tensile and compression experiments. By confirming the necessity of accounting for uncertainties with limited data, we employing the proposed framework to the real representative specimens fabricated via the LPBF method, demonstrating that the structures fabricated by LPBF have substantial uncertainty and the proposed framework is practical.

1. Introduction

Due to its high porosity and unique periodic microstructure, novel structures, including lattice structures, honeycomb structures, metamaterials, etc., are characterised by high specific strength and specific stiffness, excellent vibration absorption, noise reduction, and heat dissipation [Citation1–4]. These outstanding properties confer great application potential in various fields and received widespread attention from researchers and engineers [Citation5–7]. To fabricate novel structures with porosity and periodic microstructure, additive manufacturing (AM), especially metal AM technology, is essential [Citation8–10]. Laser powder bed fusion (LPBF) [Citation11] is a powder-based layer-by-layer metal AM process, that can produce high-density metal parts with complex shapes and precise microstructures [Citation12–14]. However, the LPBF’s quality of structures involves multiple factors [Citation15], inevitably bringing uncertainties to the manufactured structures, including size, porosity, relative density, mechanical properties, and so on [Citation16–18]. These uncertainties have a significant impact on the reliability evaluation, structural optimisation design, and improvement of manufacturing processes, and must be quantified through appropriate methods. However, due to the multiple factors involved and the high cost of testing, quantifying the uncertainties in the LPBF process becomes a challenge [Citation19, Citation20]. In particular, these uncertainties have two main characteristics, namely, the uncertainties (1) are correlated and (2) vary with certain factors. Improper modelling of the uncertainties may result in misleading reliability analysis, which can increase the risk or cost of structural applications. Therefore, to apply novel structures manufactured by LPBF to practical engineering, there is an urgent demand for a framework to quantify the uncertainties accurately [Citation21, Citation22].

The probabilistic and non-probabilistic methods are two common candidates for dealing with uncertainties. As a sophisticated approach, the probabilistic method has been deeply studied at the theoretic level and widely used to quantify various uncertainties in many engineering practices [Citation23]. The probabilistic method is very mature for uncertain problems with enough information, while in contrast, the non-probabilistic method is an important alternative for uncertainty quantification with limited sample data. In recent years, the non-probabilistic method has been widely concerned and rapidly developed. Various models concerning non-probabilistic methods have emerged in the field of uncertainty analysis. Among them, the non-probabilistic convex model [Citation24, Citation25], consisting of the multi-dimensional ellipsoid (ME) model [Citation26] and multi-dimensional parallelepiped (MP) model [Citation27], can take the correlation information into account and quantitatively describe the uncertainties using convex sets. In ME and MP models, the uncertainty domain of parameters is depicted as a multi-dimensional ellipsoid and a multi-dimensional parallelepiped, respectively. Conveniently, the degree of correlation between parameters is illustrated by the shape of the ellipsoid or parallelepiped, while the degree of uncertainty is presented by the geometry size [Citation28]. Based on the non-probabilistic convex model, many achievements have been achieved in various fields [Citation29–32], promoting the rapid development of uncertainty quantification and analysis.

The non-probabilistic convex model is suitable for quantifying uncertain-but-bounded parameters with limited sample data. At the same time, LPBF-fabricated structures involve multiple uncertainties caused by the manufacturing process and limited sample data due to high test costs. Therefore, the non-probabilistic convex model is a potentially effective approach to achieve the uncertainty quantification of LPBF-fabricated structures. Gorguluarslan et al. [Citation33] proposed a methodology utilising the Bayesian information criterion for predicting the elastic behaviour of lattice structures processed by AM. Li et al. [Citation34] presented a time-variant reliability analysis framework for predicting the lifetime of the SLM-fabricated structures with hybrid uncertainties. Lozanovski et al. [Citation35] proposed a Monte Carlo simulation-based approach to predict the stiffness of additively manufactured lattice structures, aiming at reliability analysis of AM lattice structures. To predict the reliability without the explicit model of the physics behind the manufacturing process, Snider-Simon et al. [Citation36] presented a novel workflow considering process parameters, building strategy, and test data to develop models of material microstructure. However, these studies were mainly devoted to establishing and applying reliability analysis models to LPBF-manufactured structures, while very few paid attention to developing novel uncertainty quantification and modelling approaches.

In this study, a non-probabilistic convex modelling framework is proposed to quantify uncertainties of LPBF-fabricated structures. Two types of representative structures are processed via LPBF utilising 316L and AlSi10Mg. The physical properties are tested to confirm the necessity of quantifying uncertainties with limited data. Then an efficient uncertainty quantification method is developed based on the non-probabilistic convex model. Numerical examples are provided with criteria established to evaluate the performance of the developed method. Furthermore, the proposed framework is compared with other state-of-the-art methods and subsequently applied to the LPBF fabricated representative structures.

The remainder is arranged as follows. Section 2 is devoted to developing the non-probabilistic convex modelling framework and the convex modelling processes. Section 3 establishes criteria for performance evaluation and conducts a comprehensive performance evaluation of the proposed framework. Section 4 provides comparisons with other convex modelling methods via examples and employs the proposed framework for uncertainty quantification of the LPBF-fabricated structures to verify the practicality and accuracy of the proposed framework. Subsequently, some conclusions and further discussions are given in Section 5.

2. Methods

The existing research evidently shows that structures fabricated by LPBF inherently involve uncertainties regarding physical properties. These uncertainties are challenging to be delicately depicted using traditional probabilistic models with limited experimental data. Thus, to quantitatively describe the uncertainties of LPBF-fabricated structures, a non-probabilistic convex modelling framework is proposed. As shown in , the proposed framework mainly consists of three parts, i.e. (I) Confirming structural uncertainties, (II) processing model parameters, and (III) constructing a convex model, which will be detailed in the following.

Figure 1. The proposed non-probabilistic convex modelling framework for LPBF-fabricated structures.

Figure 1. The proposed non-probabilistic convex modelling framework for LPBF-fabricated structures.

Suppose that X(s), s = 1, 2, … , p, represents p sets of sample data extracted from experiments, referring to physical properties of structures fabricated by LPBF, which will be employed to quantify the uncertain-but-bounded parameters X = {X1, X2, … , Xn}T. For the non-probabilistic convex model, these uncertain parameters can be described using an n-dimensional convex domain. Generally, the ME model is used to formulaically depict the uncertain-but-bounded parameters as shown in (a), that is. (1) ΩX={XRp|(XXm)TGE(XXm)1}(1) where ΩX represents the convex domain, and Xm = [X1m, X2m, … , Xnm] is the vector of midpoint. GE is called the characteristic matrix, which guarantees that ΩX is bounded and determines the geometric characteristic of the ellipsoid. Similarly, the uncertain space of variables also can be described by using the MP model as shown in (b), which can be formulated as (2) ΩX={XRp|[|GP(XXm)|]e}(2) where GP refers to the characteristic matrix determining the geometry of the parallelepiped and e is an n-dimensional unit vector marked as e = [1 1 … 1]T.

Figure 2. The non-probabilistic convex models: (a) ME model and (b) MP model.

Figure 2. The non-probabilistic convex models: (a) ME model and (b) MP model.

To construct the above convex models, the intervals of variables and the corresponding characteristic matrix should be acquired in advance. In most practical engineering, limited experimental samples are normally available, indicating that the intervals of variables should be appropriately determined. Based on the traditional methods and our previous work [Citation37], the midpoints of the intervals can be expressed by using the mean values, as. (3) Xim=1ps=1pXis(3) where Xis represents the experimental sample in the sth group referring to parameter Xi. The correlation coefficient between parameters, Xi and Xj, is formulated as (4) ρij=s=1p(XisXim)(XjsXjm)s=1p(XisXim)2s=1p(XjsXjm)2(4) Generally, aiming to determine the variation ranges of uncertain parameters, the convex model suitably surrounding all the sample points should be established at first. To avoid the influence of a few error data on the establishment of the convex model, accurately determining the variation ranges of uncertainties can be converted to the optimisation problem. That is, seeking the optimised convex model by adjusting or ignoring the error data. In this way, the established convex model’s geometric size is more economic and reasonable, which can minimise the impact of erroneous data. Herein, two indexes are introduced for the optimisation, including the inclusion ratio β and the cost ratio ξ, which are defined as. (5) βpin=pinp,ξ=βpinβpin1Vpin1nVpin11n(5) where p is the sample size and pin is the sample size surrounded by the convex model. βpin corresponds to the inclusion ratio when pin sample points are included, and Vpin is the volume of the convex model surrounding pin sample points. Then, the optimisation problem for searching the optimised convex model can be formulated as (6) minV,s.t.Xim,i=1,2,,n,ρij,i,j=1,2,,n,x(s)Rp,s=1,2,,p,βpinβ0,ξξ0.(6) where β0 and ξ0 are two parameter values defined according to the precision requirement. A large value of β0 means a high model accuracy, but it can also cause an increase in model volume. The parameter ξ0 reflects the balance between improving model accuracy and reducing model volume. In fact, the values of the two parameters can be adjusted according to the actual application situation. Based on the authors’ understanding and attempt of the model, it is recommended to choose the values of β0 and ξ0 as 0.95 and 0.005, respectively, to accommodate most situations. Considering that the radii of the parameter intervals determines the volume and that the ratio between the obtained interval and the actual interval of each parameter can be assumed to be approximately equal, EquationEq. (6) is equivalent to (7) minα,s.t.Xir=Xir0+αXir0,i=1,2,,n,Xim,i=1,2,,n,ρij,i,j=1,2,,n,x(s)Rp,s=1,2,,p,βpinβ0,ξξ0.(7) where α is an increment coefficient, Xir is the interval radius of the uncertain parameter Xi, and Xir0 is the initial interval radius obtained from the interval of experimental samples. EquationEq. (7) is a linear single-target optimisation problem and can be readily solved via a simple optimisation technique with linear convergence [Citation38]. Hence, the optimisation process is of high efficiency and the computation result can have high accuracy by adjusting the iterative step size in the optimisation technique.

Solving the above optimisation problem, one can identify the intervals of uncertain-but-bounded parameters, and then the convex model depicting the uncertainty domain can be mathematically given. Thus, the whole procedure of constructing the non-probabilistic convex model is summarised as follows:

Step 1: Test the physical properties of LPBF-fabricated structures to acquire the sample data x(s), s = 1, 2, … , p.

Step 2: After analysis, confirm the necessity of uncertainty quantification and identify the critical uncertain-but-bounded parameters.

Step 3: Process the data to obtain the mean value Xim and radius Xir0 of uncertain parameter Xi, i = 1, 2, … , n.

Step 4: Compute all the correlation coefficients ρij between different parameters Xi and Xj to compose the correlation matrix P.

Step 5: By solving the presented optimization problem, determine the precise interval bounds of parameters XiI.

Step 6: In light of the correlation matrix P and the intervals XiI, construct the characteristic matrix GE or GP for the corresponding convex model.

Step 7: Based on the matrix GE or GP, write the mathematical expression to establish the convex model.

At this point, the proposed non-probabilistic framework can be fully established to measure the uncertainty of LPBF-fabricated structures. It should be noted that the proposed framework can obtain precise variation intervals of uncertain parameters based solely on limited actual data, and achieve the removal of error samples during the modelling process.

3. Performance evaluation

3.1.‏ Criteria establishment

To quantitatively evaluate the practical performance of the proposed framework, several criteria are established based on our previous work [Citation37], including the prediction accuracy η reflecting the predictive performance of modelling methods for unknown data, volume ratio ζ and standard volume ratio ζ¯ indicating the economic benefits of modelling methods, (8) η=NSNT×100%,ζ=VCVR×100%,ζ¯=ζ1n(8) where NS is the sample size of test data in the established convex model, and NT is the total sample size of test data. VC and VR represent the volumes of the established convex model and the corresponding hyper-rectangle model, respectively. The specific calculation of VC and VR can be referred to [Citation39]. Generally, an excellent convex model is expected to have high prediction accuracy with a low standard volume ratio. That is, to obtain a convex model with high accuracy at a low cost in engineering. In this regard, a new criterion for comprehensively evaluating convex models can be defined as (9) Q=ηζ¯(9) where Q is the new criterion called cost performance. It can be observed from EquationEq. (9) that a considerable value of Q represents an outstanding performance of a convex model containing both the prediction accuracy and standard volume ratio.

3.2. Performance evaluation

With the established criteria, it is convenient to concretely evaluate the performance of the convex modelling method under various conditions. Considering the potential situations in practical engineering, the sample data can be of different numbers, distributions, correlations, and even incorrect samples. Therefore, the capability of the proposed method in the three cases should be tested.

Firstly, to test the capability of the proposed method with different numbers of sample data, randomly generate p two-dimensional sample data from two uncertain variables, X1 and X2, for uncertainty quantification. Herein the value of p is assumed to be an integer from 10 to 90 to supply nine cases. Suppose the variables X1 and X2 obey the normal distribution with mean values μX1=μX2=100, and deviations σX1=σX2=10. The correlation coefficient is set as ρ =  0.5. By using the Pauta criterion [Citation40], the interval of the variable obeying the normal distribution can be expressed as [μ−3σ, μ+3σ], that is [70, 130] for variables X1 and X2, which makes it easy to calculate the volume of the corresponding hyper-rectangle model. To balance the calculation efficiency and accuracy, the total sample size of the test data NT is set as 10,000, and the mean value of 100 test results is accepted in each case.

shows the performance of the established ellipsoid model under different sample sizes. It implies that even in small sample sizes, the established ellipsoid model can have superior performance, e.g. the prediction accuracy η = 77.65% under the condition p = 10 and η = 92.82% under the condition p = 30. Specifically, the prediction accuracy rises as the sample number increases and ultimately approaches 100%. The standard volume ratio increases with the sample size but remains below 100%, indicating that the space of the established model is smaller than that of the corresponding hyper-rectangle. In addition, under the combined effect of variations in prediction accuracy and standard volume ratio, the cost performance gradually decreases with the increase of the sample number but is greater than one. Thus, the proposed convex modelling method possesses outstanding performance when the sample data is limited.

Figure 3. Performance under different sample numbers.

Figure 3. Performance under different sample numbers.

Secondly, different correlations between two uncertain variables are considered to further study the performance of the proposed modelling method. Suppose that the two random variables X1 and X2 are generated under the condition that the correlation coefficient ρ are the following cases: (Ⅰ) ρ = 0.1; (Ⅱ) ρ = 0.2; (Ⅲ) ρ = 0.3; (Ⅳ) ρ = 0.4; (Ⅴ) ρ = 0.5; (Ⅵ) ρ = 0.6; (Ⅶ) ρ = 0.7; (Ⅷ) ρ = 0.8; (Ⅸ) ρ = 0.9. Similarly, the ellipsoid model is established by randomly employing 30 samples, and then 10,000 sample points are randomly created for performance testing. In each case, the mean value of 100 test results is adopted.

presents the test results of the established ellipsoid model under different correlations. It can be noticed that when other conditions remain unchanged, the correlation coefficients of variables will have a significant impact on the ellipsoid model, e.g. ζ¯ = 66.62% and Q = 1.40 when ρ = 0.1, and ζ¯ = 27.26% and Q = 3.50 when ρ = 0.9. In particular, while the fluctuation in prediction accuracy is not evident, the standard volume ratio and cost performance are markedly changed. The standard volume ratio decreases visibly with the correlation increasing, while the cost performance rises sharply as the correlation enhances. Consequently, the proposed convex modelling method can effectively handle uncertain variables with correlation, especially those with high correlation.

Figure 4. Performance under different correlations.

Figure 4. Performance under different correlations.

Finally, uncertain variables subject to two types of distribution, that is normal and uniform distributions, are discussed to evaluate the prediction capability. Assume that the centres and deviations of the normal distribution remain unchanged, and the uncertainty range of the uniform distribution is set as [90, 110]. The number of samples is p = 30, and the correlation coefficient is ρ = 0.5. Equally, 10,000 sample points are generated for testing, and the mean value of 100 test results is adopted in each condition.

The test results are presented in , in which the prediction accuracy of all established convex models exceeds 92%, and the standard volume ratio is less than one. Thus, it manifests that the proposed convex modelling method owns excellent performance in both the two kinds of distributions, demonstrating that the proposed convex modelling method possessing excellent generalisation ability.

Table 1. Test results under different sample distributions.

At the end of this subsection, it is worth emphasising that the established convex models can ignore some marginal sample points during the modelling process in the tests, which demonstrates the capability of preprocessing error data of the proposed method.

3.3. Efficiency and accuracy

The efficiency of the proposed framework mainly depend on modelling process, especially the calculation of the optimisation problem in EquationEq. (7), while other processes occupy little time. Without considering error sample points, the optimisation problem can be solved with linear convergence via the advanced-retreat method. The total number of the computational effort is q × l, where q is the number of experimental samples, l is the number of iterative steps.

In addition to the influencing factors analyzed in Section 3.2, the accuracy of uncertainty quantification in the proposed framework largely relates to the iterative step-size for solving the optimisation problem. The actual interval radius Xir must be between two iterative steps, as. (10) Xir0+(l1)μXir0<XirXir0+()Xir0,i=1,2,,l(10) where μ is the iterative step-size coefficient. According to EquationEq. (10), the accuracy of the solution satisfies the inequality written as (11) βa<[Xir0+()Xir0][Xir0+(l1)μXir0]Xirμ(11) Thus, it can be observed that a small value of μ can achieve high accuracy of the solution. However, it also increases the number of iterative steps, which inevitably affects the computing efficiency. To balance the efficiency and accuracy of the solution, μ is generally recommended be to set to 0.01. In practical applications, the value of μ can be adjusted based on accuracy and efficiency requirements.

4. Results and discussions

To further verify the effectiveness of the proposed convex modelling framework, we will systematically compare the model established by the proposed framework with other advanced methods through benchmark numerical examples. Herein, two existing competitive convex models, namely the convex correlation coefficient-based (CCC-based) model and the sample correlation coefficient-based (SCC-based) model [Citation39], are adopted. The CCC-based model heavily relies on the marginal sample points, while the SCC-based model focuses on the information of all samples. Therefore, these two models have advantages in different situations and are suitable for comparison with the new model. Then, through processing and testing of the practical structures, a complete uncertainty quantification process is conducted around the proposed framework for the LPBF-fabricated structures.

4.1. A two-dimensional uncertainty problem

A two-dimensional (2D) uncertainty quantification problem related to LPBF- fabricated structure is presented to validate the developed convex modelling method before embedding it into the proposed framework. Two uncertain variables X1 and X2 with their correlation ρ = 0.5 are considered to be described by using convex models with given 50 groups of samples. The 50 groups of samples are randomly generated in the intervals X1I = [90,110] and X2I = [90,110] with obeying uniform distribution, and the correlation between the two variables ρ = 0.5, as displayed in .

Table 2. Samples of X1 and X2 for convex modelling.

Applying the proposed method for uncertainty quantification, the mean values and radii of the two parameters can be acquired as X1m=99.73, X2m=99.93 and X1r0=7.76, X2r0=7.25. Then calculating the correlation coefficient and the correlation matrix P can be written as. (12) P=[10.33040.33041](12) Utilising the mean values, radii, and correlation matrix to model the optimisation problem and solve it to acquire the precise variation intervals of the parameters as X1I=[91.43,108.03] and X2I=[92.17107.69]. Based on the correlation matrix and variation intervals, the characteristic matrix GE or GP can be constructed. Finally, the ellipsoid model and the parallelepiped model quantifying the uncertain parameters can be comfortably constructed. And for comparison, the CCC-based model and the SCC-based model are also established. intuitively shows the two types of convex models for describing the uncertainty using different modelling methods. provides the key parameters of the convex models with t being the time consumption for convex modelling.

Figure 5. Convex models: (a) Ellipsoid models and (b) Parallelepiped models.

Figure 5. Convex models: (a) Ellipsoid models and (b) Parallelepiped models.

Table 3. Parameters related to the performance of the models.

It can be found that, based on the given 50 samples, the model constructed by the proposed method has a smaller volume while enclosing all the provided samples, with its better performance demonstrated compared with the others. Additionally, in terms of time consumption, the outstanding modelling efficiency of the proposed method is also revealed. Therefore, this 2D problem has confirmed the suitability and accuracy of the proposed method for uncertainty problems with limited data.

4.2. A cantilever beam

Consider a typical three-dimensional cantilever beam, as shown in , where its free end is subjected to a combined action of a concentrated horizontal force Fx = 50,000N and a concentrated vertical force Fy = 25,000N. To ensure the load-bearing safety, the maximum stress on the beam must be less than the yield stress σS. Based on the knowledge of mechanics, the maximum stress of the cantilever beam occurs at its fixed end. The limit state equation can be expressed as. (13) g(b,w,l)=σS6Fxlw2h6Fylwh2(13) where l, w and h are the length, width and height of the cantilever beam, respectively. Due to the existence of processing errors, the geometric dimensions of the cantilever beam are not fixed values in actuality but fluctuate within a small range. Thus, the geometric parameters should be treated as uncertain variables and appropriate uncertainty quantification need to be conducted. Herein, 34 samples containing two error samples far from the centre are available, as listed in .

Figure 6. A cantilever beam.

Figure 6. A cantilever beam.

Table 4. Samples of geometric parameters of the cantilever beam [Citation41].

Firstly, applying the proposed method to establish the convex model for uncertainty quantification, the mean values and radii of the uncertain parameters can be obtained as wm=99.52mm, hm=199.22mm and lm=997.21mm and wr0=17.39mm, hr0=20.19mm and lr0=201.04mm. Then we calculate the correlation coefficients between the three parameters in pairs to form the correlation matrix P, which can be written as. (14) P=[10.02850.29730.028510.02030.29730.02031](14) Based on the mean values, radii, and correlation matrix of the parameters, modelling the optimisation problem and solving it to determine the precise interval bounds of parameters. Herein, the variation intervals of the geometric parameters can be acquired as wI=[90.16,109.42]mm, hI=[181.06,217.16]mm and lI=[902.26,1085.56]mm. According to the correlation matrix and the acquired variation intervals, the characteristic matrix GE or GP can be constructed. Finally, the ME model and MP model quantifying the geometric parameters with uncertainties can be mathematically formulated.

The ME model can be expressed as. (15) [(w99.79)/9.63(h199.11)/18.05(l993.91)/87.11]T[10.02850.29730.034210.02030.29730.02031]1[(w99.79)/9.63(h199.11)/18.05(l993.91)/87.11]1(15) The MP model can be expressed as (16) [|[0.85650.01310.13040.01480.97410.01110.13080.00990.8593]1[(w99.79)/9.63(h199.11)/18.05(l993.91)/87.11]|][111](16) To visually display the bounding effect of the established convex models in this example, and show the position and shape information of the ME model and the MP model, respectively.

Figure 7. Projections of the ME model: (a) w-h plane; (b) w-l plane and (c) h-l plane.

Figure 7. Projections of the ME model: (a) w-h plane; (b) w-l plane and (c) h-l plane.

Figure 8. Projections of the MP model: (a) w-h plane; (b) w-l plane and (c) h-l plane.

Figure 8. Projections of the MP model: (a) w-h plane; (b) w-l plane and (c) h-l plane.

provides the key parameters of convex models established via different methods to facilitate a detailed comparison of various models. Herein, κ is the sample coverage rate, which is the ratio of samples included in the model to the total samples. From , we can observe that the centres of uncertainty domains represented by different models are approximate. In terms of modelling efficiency, the proposed method is faster than the CCC-based method and is similar to the SCC-based method. As for the sample coverage rate and volume of the convex models, the proposed method maintains a high sample coverage rate with a pleasurable volume size. In addition, we highlight that the proposed method has successfully removed the two edge data as erroneous data during modelling, while the other two methods overlook the erroneous samples. Therefore, we can conclude from this numerical example that the proposed method can construct convex models with superior comprehensive performance and efficiently provide accurate solutions.

Table 5. Key parameters of different convex models.

4.3. LPBF-fabricated structures

4.3.1. Design and fabrication of the tested structures

Two types of representative structures, solid and lattice structures, are designed and fabricated using LPBF technology for tensile and compression experiments, as shown in . The lattice structure used as the compression specimen is a triply periodic minimal surface (TPMS) porous structure composed of 4 × 4 × 4 unit cells with a size of 40 × 40 × 40 mm, which possess excellent compression and energy absorption effect due to its internal porous structure. The solid structure used as the tensile specimen is a standard specimen with a total length of 170 mm and a width of 10 mm. 316L stainless steel and AlSi10Mg aluminium alloy are utilised to fabricate the structures. The details about the chemical composition of the two raw materials used for printing are tested and shown in and . The particle size distribution of spherical powders for both materials is 15 µm to 53 µm, with a median particle size of 32.7 µm for 316L material and 38 µm for AlSi10Mg material. The apparent density of 316L stainless steel spherical powder is 4.18 g/cm3 and the flowability defined by the Hall flowmeter is 18 s/50 g. And the apparent density of AlSi10Mg aluminium alloy spherical powder is 1.36 g/cm3 and the flowability is 65.8 s/50 g.

Figure 9. Two representative structures fabricated by LPBF: (a) Solid structure and (b) lattice structure.

Figure 9. Two representative structures fabricated by LPBF: (a) Solid structure and (b) lattice structure.

Table 6. The chemical composition of the 316L stainless steel powder.

Table 7. The chemical composition of the AlSi10Mg aluminium alloy powder.

The LPBF process is conducted on a DiMetal-100 SLM machine developed by the South China University of Technology. All the manufacturing processing occurs in a nitrogen environment where the O2 content is less than 0.05%, and the dust removal rate is greater than 95%. The detailed LPBF processing parameters used by the DiMetal-100 machine are summarised in . The printing direction of AM process is shown in . The solid structure sample is printed vertically along the X direction, and the lattice structure sample is normally stacked and printed on the XY plane.

Figure 10. The building direction of the structure samples on the powder bed.

Figure 10. The building direction of the structure samples on the powder bed.

Table 8. The processing parameters used by the LPBF.

4.3.2. Experiments for testing physical properties

shows the printing results of two representative structures via LPBF. (a) and (b) are solid structure samples printed using 316L and AlSi10Mg materials, respectively; (c) and (d) are the lattice structure samples printed using 316L and AlSi10Mg material, respectively. Due to the LPBF involving a series of coupled physical phenomena, the process-structure–property relationship is extremely complex. The mechanical properties of the printed parts are directly determined by the microstructure, and also considerably affected by the residual stress. Therefore, the inherently uncertain performance of the LPBF-fabricated structures mainly stems from the microstructure and residual stress. The mechanical properties exhibited by the printed macro-scale structure directly reflect the comprehensive influence of the microstructure and residual stress. From this perspective, analyzing the uncertain mechanical properties of the macro-scale structure can verify the inherent uncertainty in the comprehensive performance of the LPBF-fabricated structure.

Figure 11. Specimens fabricated by LPBF for experiments: (a) 316L solid structures; (b) AlSi10Mg solid structures; (c) 316L lattice structures; (d) AlSi10Mg lattice structures.

Figure 11. Specimens fabricated by LPBF for experiments: (a) 316L solid structures; (b) AlSi10Mg solid structures; (c) 316L lattice structures; (d) AlSi10Mg lattice structures.

Firstly, to confirm the uncertainty of LPBF-fabricated structures, the mass and density of the 50 solid samples with AlSi10Mg material are tested. It is found that the mass of the sample specimen is between 7.289 and 7.654 g, and the density is between 3.0618 and 3.2149 g/m3, qualitatively indicating that there are indeed significant uncertainties in LPBF-fabricated structures. Then, we measure the mechanical properties of the 316L specimens by conducting several experiments. During the experiments, the displacement change is read using an extensometer, and the force value is recorded by a universal testing machine. The stress–strain curve is calculated by comparing each determined displacement value and its corresponding force value in the experimental data. The load range applied in the tensile test is 0∼5540 N, while it is 0∼73456 N before the densification stage in the compression test. presents the final states of the LPBF-fabricated structures after performing the experiments, while gives the corresponding stress–strain curves. It can be found that there is not much difference in appearance among the structures manufactured by LPBF, but there are significant differences in mechanical properties. For example, in tensile tests, the fracture of solid structures is located at different positions, and there are certain differences in the stress–strain curves of each solid structure. To quantify the differences among LPBF-fabricated structures, we conduct comprehensive experiments on a total of 49 samples of the 316L solid structure to measure the density, weight, elastic modulus, yield strength, and tensile strength. Finally, 34 sets of effective data are obtained as shown in . The physical parameters of these structures obviously fluctuate within a certain range, which can significantly influence the engineering application of structures. Additionally, the physical parameters of the 5 lattice structure samples, including the density, weight, elastic modulus and compressive strength, also exhibit fluctuations as shown in . Therefore, accounting for uncertainties of structures manufactured by LPBF with limited data is of necessity and urgency.

Figure 12. Final states of the specimens fabricated by LPBF: (a) 316L solid structures in tensile tests; (b) 316L lattice structures in compression tests.

Figure 12. Final states of the specimens fabricated by LPBF: (a) 316L solid structures in tensile tests; (b) 316L lattice structures in compression tests.

Figure 13. Stress-strain curves of specimens fabricated by LPBF: (a) 316L solid structures in tensile tests; (b) 316L lattice structures in compression tests.

Figure 13. Stress-strain curves of specimens fabricated by LPBF: (a) 316L solid structures in tensile tests; (b) 316L lattice structures in compression tests.

Table 9. Physical parameters of the 316L solid structures from tensile experiments.

Table 10. Physical parameters of the 316L lattice structures from compression experiments.

4.3.3. Uncertainty quantification

Herein, in light of the experimental data related to the physical parameters of the 316L solid structures in , we can apply the proposed convex modelling method to quantify the structural uncertainties. By adopting the corresponding ellipsoid model, the uncertainties of parameters can be mathematically quantified as. (17) [(E167379)/10014(σS312)/57(σb530)/73(W17.924)/0.715(D7.529)/0.300]T[10.35930.50780.07820.07960.359310.85960.20960.21000.50780.859610.26110.26230.07820.20960.261111.0000.07960.21000.26231.0001]1[(E167379)/10014(σS312)/57(σb530)/73(W17.924)/0.715(ρ7.529)/0.300]1(17) where E, σS and σb are the elastic modulus, yield strength and tensile strength, respectively. W is the weight and D is the density. From the correlation matrix, it can be noted that the correlations between various parameters are different. Among them, the correlation between E and W is very small, only 0.0782, revealing that the two parameters correlate less. However, interestingly, the correlation between W and D is equal to 1, indicating a direct correlation between the two parameters, which is consistent with our common sense as density can be calculated by weight and proves the accuracy of the established convex model. To provide more intuitive information about uncertainties described in the model, displays the corresponding variation intervals, centres, and radii for each parameter. Considering the importance of porosity formed by the microstructure in LPBF-fabricated structures, the ratio of density’s deviation to the median is used as an indicator to quantitatively evaluate the uncertainty. Thus, according to the uncertainty quantification results of the proposed method, the uncertainty indicator of the LPBF-fabricated solid structure can be marked as 3.98%.

Table 11. Variation intervals of physical parameters of LPBF-fabricated solid structures.

Similarly, according to the sample data from the compression experiment of the LPBF-fabricated lattice structure in , the proposed method can be used to quantify the uncertainties. By adopting the proposed convex modelling method, the ellipsoid model for uncertainty quantification of parameters can be expressed as. (18) [(E17.2)/0.2(σC330.0)/3.7(W109.239)/0.471(D8.12)/0.03]T[10.71040.96610.95670.710410.81810.79440.96610.818110.99770.65670.79440.99771]1[(E17.2)/0.2(σC330.0)/3.7(W109.239)/0.471(D8.12)/0.03]1(18) where σC is the compressive strength. From the correlation matrix, it can be found that apart from the consistent correlation between W and D, the correlation between parameters of lattice structures is significantly different from that of solid structures. For example, the correlation between E and W reaches 0.9661, indicating a strong correlation between these two parameters. This completely different result from the solid structure is essentially caused by the internal microstructure of the lattice structure. Therefore, the established correlation matrix is reasonable. shows the variation intervals, centres, and radii for each parameter. Correspondingly, the uncertainty indicator of the LPBF-fabricated lattice structure can be calculated as 0.37% based on the results of the proposed method. This is smaller than the uncertainty indicator of the solid structure, indicating that the fluctuation of its density is relatively stable, that is, the change in porosity is small.

Table 12. Variation intervals of physical parameters of LPBF-fabricated lattice structures.

Combining and , it can be seen that although the small amount of data from the compression test can have a certain impact on the result, it does not affect the good application of the model. Furthermore, it is worth noting that during the modelling process of structural compression test data using the proposed method, the fourth set of test data was automatically removed. If not removed, the uncertainty intervals of the obtained parameters are very large, such as EI=[14.1,20.2]MPa, σCI=[245.1,413.4]MPa, which is unreasonable and meaningless.

With the acquired information on the LPBF-fabricated solid structure and lattice structure, we have achieved measurement of various uncertain variables using the proposed method, further verifying the effectiveness of the uncertainty modelling framework proposed in this paper.

5. Conclusions

Owing to the complicated manufacturing process of LPBF-fabricated structures, the processing tolerance inevitably exists, and the sample data is limited, resulting in the difficulty of dealing with uncertainties. To efficiently and exactly quantify the uncertainties of structures fabricated by LPBF with limited data, we have proposed a non-probabilistic convex modelling framework. By applying the proposed framework, the constructed convex models can accurately enclose the sample points concerning uncertain parameters with high efficiency and superior cost performance. We have established critical criteria and comprehensively investigated the application performance of the proposed method via test standards and comparison. We conclude that the proposed non-probabilistic convex modelling framework not only offers new opportunities for applying convex models to LPBF-fabricated structures with limited data but also provides a deeper understanding of the characteristics of convex models that can be particularly important. The proposed strategy is promising to provide theoretical guidance for the precise characterisation of the properties of LPBF-fabricated high-performance structures. Of course, the proposed convex modelling method also has some limitations, such as the inability to display the probability distribution of variables due to being a convex model based on limited samples, and the acquired variable intervals may not be accurate due to the significant influence of the limited samples. In future work, we will improve our modelling methods and discuss the quantitative analysis of uncertainty in the fabricating process of structures from multiple dimensions, such as material properties, preparation process, measurement errors, and numerical solutions. We will specifically analyze and measure the hardness, roughness, and residual stress of the LPBF-fabricated structure to describe its integrity.

CRediT authorship contribution statement

G. Zhao: Writing-original draft, Conceptualisation, Formal analysis, Investigation, Methodology, Supervision. R. Wang: Conceptualisation, Investigation, Validation, Data curation. F. Li: Methodology, Investigation. J. Liu: Writing-review & editing, Funding acquisition, Project administration, Methodology, Supervision.

Acknowledgements

Thanks very much to the reviewers for their comments on the paper.

Data availability

Data available on request from the authors.

Disclosure statement

No potential conflict of interest was reported by the author(s).

Additional information

Funding

This work was supported by National Natural Science Foundation of China: [grant no 12172095]; Guangzhou Science and Technology Planning Project: [grant no 202201020193;202201010399]; Anhui Provincial Department of Education: [grant no KJ2021A0157].

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