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Inorganic and Nano-Metal Chemistry Volume 50, 2020 - Issue 8
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Articles

Influence of CaF2 on the preparation of ZnO via SHS method

Qiyu WangDepartment of Materials Engineering, Wuhan University, Wuhan, P. R. ChinaView further author information
,
Chu ZhangDepartment of Materials Engineering, Wuhan University, Wuhan, P. R. ChinaView further author information
,
Hui ZhangDepartment of Materials Engineering, Wuhan University, Wuhan, P. R. ChinaView further author information
&
Guodong ZhangDepartment of Materials Engineering, Wuhan University, Wuhan, P. R. ChinaCorrespondence[email protected]
View further author information
Pages 587-591 | Received 08 Apr 2017, Accepted 27 Aug 2019, Published online: 16 Jun 2020
 
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Abstract

A closing synthesis device with special structure was designed to effectively collect the ZnO synthesized via self-propagating high temperature synthesis (SHS) method. With this device, the influence of CaF2 on products was investigated. Products were characterized using scanning electron microscope (SEM) and X-ray diffraction (XRD). Results showed that with the increase of CaF2, there is a trend of first increase and following decrease in the yield of products and there appears increasing amount of one-dimensional ZnO nanostructures and there are no obvious changes on the structure of products. Possible mechanisms of the influence of CaF2 on products were discussed.

Additional information

Funding

This work is supported by Nanotechnology Special Fund of Suzhou (ZXG201447) and Natural Science Foundation of Hubei Province (2014CFB707).

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