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Original Articles

SOLID-PHASE MICROEXTRACTION DETERMINATION OF ALCOHOL USING PENCIL LEAD*

, &
Pages 627-634 | Received 17 Oct 2000, Accepted 30 Nov 2000, Published online: 02 Feb 2007
 

Abstract

In order to conquer the shortcomings of commercial SPME coatings: they can’t stand high temperature, are easy to drop off, the longevity of usage is short and they are too expensive, we used pencil lead as a new sorbent to analyze the alcohol in water. The linear range is 5×10−6−2.5×10−8g/mL. The detection limit is 5×10−9g/mL. We also used this method to determine the concentration of alcohol in environment water. The recoveries are 107.5% and 97%. The RSD is 5.9%. Hence the pencil lead is a very good material for solid-phase microextraction (SPME).

* Nature science fund project in Hu Bei province.

Acknowledgments

Notes

* Nature science fund project in Hu Bei province.

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