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Journal of Carbohydrate Chemistry Volume 23, 2004 - Issue 8-9
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Original Articles

A Total Synthesis of a New Class of Biazine Thioglycosides

Galal H. Elgemeie Chemistry Department, Faculty of Science, Helwan University, Ain‐Helwan, Cairo, Egypt
,
Mona M. Hussein Chemistry Department, Faculty of Science, Cairo University, Giza, Egypt
&
Sheakha A. Al‐Khursani Chemistry Department, Girls College of Science, Dammam, Kingdom of Saudi Arabia
Pages 465-481 | Published online: 09 Aug 2006
 
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Abstract

A new method for the synthesis of bipyridinyl S‐glycosides 11 and 12 has provided the title compounds in a higher yield. Application of a one‐pot glycosylation methodology resulted in an efficient, high‐yield synthesis of biazine S‐glycosides 17–20 An X‐ray diffraction analysis of 11 disclosed the conformation of this glycoside as the S‐glycoside and not the corresponding N‐form.

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