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Journal of Liquid Chromatography & Related Technologies Volume 26, 2003 - Issue 8
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Original Articles

Application of Alkylamide Phase to the Separation of Inorganic Anions by Reversed Phase HPLC

Bogusław Buszewski Department of Environmental Chemistry & Ecoanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina. 7, Torun, P1‐87 100, PolandCorrespondence[email protected]
,
Tadeusza Buszewska Chemical Education Laboratory, Faculty of Chemistry, Nicolaus Copernicus University, Torun, Poland
&
Renata Gadzała‐Kopciuch Department of Environmental Chemistry & Ecoanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina. 7, Torun, P1‐87 100, Poland
Pages 1197-1206 | Received 01 Dec 2002, Accepted 02 Jan 2003, Published online: 06 Feb 2007
 
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Abstract

Packing with an alkylamide chemically bonded stationary phase (AP) for high performance liquid chromatography (HPLC) was applied for the determination of inorganic anions in water samples. The conventional octadecyl (C18) stationary phase was used as a reference column packing material for reversed‐phase (RP) HPLC. The mobile phase composition under ion‐pair RP HPLC conditions, was optimized by changing the concentration of the organic modifier (acetonitrile), the ionic strength of eluent (addition of TRIS), and the pH value. The data obtained were used for qualitative and quantitative determination of anions in samples of drinking water and water from the Vistula River.

Acknowledgment

This work was supported by the European Union, project EuroCat‐VisCat No. EVK1‐CT‐2000‐00044.

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