Abstract
Three polysaccharide‐based chiral stationary phases (CSPs), including cellulose‐tris‐(3,5‐dimethylphenylcarbamate) (CDMPC), cellulose‐tris‐(phenylcarbamate) (CMPC), and amylose‐tris‐(3,5‐dimethylphenylcarbamate) (ATPC) were synthesized. The successful resolution of six pesticides and related intermediates on these CSPs, by applying n‐hexane:isopropyl alcohol mobile phase, is described. The influence of isopropyl alcohol concentration in mobile phase was also studied.