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Journal of Liquid Chromatography & Related Technologies Volume 28, 2005 - Issue 2
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Original Articles

Chiral Separation of β2‐Blockers on Pirkle‐Type Chiral Stationary Phases

Dandan Zhang Department of Analytical Chemistry, Shenyang Pharmaceutical University, P.R. China
,
Famei Li Department of Chemistry and Chemistry Institute for Functional Materials, Pusan National University, Busan, 609‐735, Korea
&
Myung Ho Hyun Department of Chemistry and Chemistry Institute for Functional Materials, Pusan National University, Busan, 609‐735, KoreaCorrespondence[email protected]
Pages 187-198 | Received 15 Aug 2004, Accepted 19 Sep 2004, Published online: 22 Aug 2007
 
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Abstract

Liquid chromatographic resolution of six racemic β2‐blockers including bambuterol, clenbuterol, clenpropol, fumoterol, mabuterol, and terbutaline was studied on two Pirkle‐type chiral stationary phases (CSPs) such as α‐Burke‐2 and Pirkle‐1J. By varying the mobile phase compositions, five of the six β2‐blockers were successfully resolved on α‐Burke‐2 CSP, while only two β2‐blockers were resolved on Pirkle‐1J CSP.

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