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Nucleosides, Nucleotides & Nucleic Acids Volume 20, 2001 - Issue 8
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Original Articles

CONVENIENT METHOD FOR THE PREPARATION OF 2′-DEOXYRIBOSYLUREA BY THYMIDINE OXIDATION AND NMR STUDY OF BOTH ANOMERS

Igor Dubey Institute of Molecular Biology and Genetics, National Academy of Sciences, Kyiv, Ukraine
,
Genevie`ve Pratviel
,
Anne Robert
&
Bernard Meunier
Pages 1463-1471 | Received 09 Sep 2000, Accepted 30 Dec 2000, Published online: 17 Aug 2006
 
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Abstract

The synthesis of 2′-deoxyribosylurea by thymidine oxidation with potassium permanganate followed by alkaline hydrolysis of intermediates is described. The anomeric configuration of the resulting products was studied by NMR spectroscopy.

ACKNOWLEDGMENTS

I. D. is indebted to the Université Paul Sabatier (Toulouse) for a fellowship. Yannick Coppel (LCC-CNRS) is gratefully acknowledged for performing the ROESY experiments.

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