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Nucleosides, Nucleotides & Nucleic Acids Volume 21, 2002 - Issue 6-7
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Original Articles

FORMATION OF 2′-DEOXY-2-NITROADENOSINES BY REACTION OF 2′-DEOXYADENOSINES WITH COPPER(II) NITRATE/ACETIC ANHYDRIDE

Toyo Kaiya Graduate School of Pharmaceutical Sciences, Nagoya City University, Tanabedori, Mizuho-ku, Nagoya, 467-8603, Japan
,
Haruko Tanaka Graduate School of Pharmaceutical Sciences, Nagoya City University, Tanabedori, Mizuho-ku, Nagoya, 467-8603, Japan
&
Kohfuku Kohda Graduate School of Pharmaceutical Sciences, Nagoya City University, Tanabedori, Mizuho-ku, Nagoya, 467-8603, JapanCorrespondence[email protected]
Pages 427-433 | Received 11 Mar 2002, Accepted 28 May 2002, Published online: 31 Aug 2006
 
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ABSTRACT

Nitration of 9-substituted [ethyl, (Ac)2-2′-deoxyribosyl, (Ac)3-ribosyl] N 6-acetyladenine derivatives with Cu(NO3)2·3H2O/Ac2O was examined. Nitration proceeded at the 2-position, although the yield was low. Removal of the acetyl groups gave 2′-deoxy-2-nitroadenosine derivatives.

ACKNOWLEDGMENT

We thank Dr. R. Taguchi for ESI mass analyses.

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