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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 6
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Original Articles

NEW HALOGENATION REAGENT SYSTEM FOR ONE-POT CONVERSION OF ALCOHOLS INTO IODIDES AND AZIDES*

Ahmed Kamal Division of Organic Chemistry, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
G. Ramesh Division of Organic Chemistry, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
N. Laxman Division of Organic Chemistry, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 827-833 | Received 27 Mar 2000, Published online: 09 Nov 2006
 
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Abstract

In situ generation of hydrogen iodide from methanesulphonic acid/sodium iodide in different solvents was found to be an attractive reagent system for the chemoselective conversion of various alcohols to their corresponding iodides. Moreover, treatment of benzylic and allylic alcohols with this reagent system, followed by substitution with azide ion, produced the corresponding azides in one pot in good yields.

*IICT Communication No. 4529.

ACKNOWLEDGMENTS

NL is thankful to CSIR (New Delhi) for the award of a Senior Research Fellowship.

Notes

*IICT Communication No. 4529.

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