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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 10
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Original Articles

SYNTHESIS OF 4-DEOXYCARBAZOMYCIN B: A CONVENIENT ALTERNATIVE

Bejoy K. Chowdhury Department of Chemistry, School of Tropical Medicine, Calcutta, 700073, India
&
Shailendra Jha Department of Chemistry, Presidency College, 86/1 College Street, Calcutta, 700073, India
Pages 1559-1564 | Received 03 Aug 2000, Published online: 02 Aug 2010
 
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Abstract

4-Deoxycarbazomycin B(3) was synthesized by condensation of 4-methoxy-2,3-dimethylacetanilide (8) with bromobenzene in presence of cuprous iodide and potassium carbonate, and subsequent hydrolysis with 20% aqueous ethanolic KOH, followed by cyclisation of the resulting substituted diphenylamine (9) with palladium acetate in acetic acid.

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