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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 13
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Original Articles

SOLVENT FREE BECKMANN REARRANGEMENT OF KETOXIMES BY ANHYDROUS FERRIC CHLORIDE

M. M. Khodaei Department of Chemistry, Razi University, Kermanshah, Iran
,
F. A. Meybodi Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
,
N. Rezai Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
&
P. Salehi Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
Pages 2047-2050 | Received 13 Sep 2000, Published online: 09 Nov 2006
 
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Abstract

Beckmann rearrangement of ketoximes is achieved efficiently by anhydrous FeCl3 in the absence of solvent. Unsymmetrical oximes are selectively produced one of the two possible products in good yields. Similar reactions are not occurred in the presence of solvent.

ACKNOWLEDGMENT

We are grateful to Razi University Research Council for financial support of this work.

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