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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 14
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Original Articles

A SHORT PROCEDURE FOR SYNTHESIS OF 4-ETHYNYL-2,2,6,6-TETRAMETHYL-3,4-DEHYDRO-PIPERIDINE-1-OXYL NITROXIDE

Peter M. Gannett School of Pharmacy, West Virginia University, Basic Pharmaceutical Sciences, P.O. Box 9530, Morgantown, West Virginia, 26506-9530, U.S.A.
,
Eva Darian School of Pharmacy, West Virginia University, Basic Pharmaceutical Sciences, P.O. Box 9530, Morgantown, West Virginia, 26506-9530, U.S.A.
,
Jeannine H. Powell School of Pharmacy, West Virginia University, Basic Pharmaceutical Sciences, P.O. Box 9530, Morgantown, West Virginia, 26506-9530, U.S.A.
&
Edward M. Johnson School of Pharmacy, West Virginia University, Basic Pharmaceutical Sciences, P.O. Box 9530, Morgantown, West Virginia, 26506-9530, U.S.A.
Pages 2137-2141 | Received 12 Oct 2000, Published online: 09 Nov 2006
 
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Abstract

The spin-probe labeling technique has been applied to DNA and offers the possibility of studying antisense agents in cells. Simpler syntheses of spin-probes for incorporation into DNA would facilitate this. Here, we describe the synthesis of a new spin probe that requires half the number of steps of related 5 ring nitroxide.

ACKNOWLEDGMENTS

We thank the NIH for their financial support of this work (15GM57630-01).

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