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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 14
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Original Articles

SYNTHESIS OF AMINONAPHTHALENE DERIVATIVES USING THE BUCHERER REACTION UNDER MICROWAVE IRRADIATION

Alvaro Cañete Department of Organic Chemistry and Physical Chemistry, Faculty of Chemical and Pharmaceutical Sciences, University of Chile, Casilla 233, Santiago 1, Chile
,
Mónica X. Meléndrez Department of Organic Chemistry and Physical Chemistry, Faculty of Chemical and Pharmaceutical Sciences, University of Chile, Casilla 233, Santiago 1, Chile
,
Claudio Saitz Department of Organic Chemistry and Physical Chemistry, Faculty of Chemical and Pharmaceutical Sciences, University of Chile, Casilla 233, Santiago 1, Chile
&
Antonio L. Zanocco Department of Organic Chemistry and Physical Chemistry, Faculty of Chemical and Pharmaceutical Sciences, University of Chile, Casilla 233, Santiago 1, ChileCorrespondence[email protected]
Pages 2143-2148 | Received 12 Oct 2000, Published online: 09 Nov 2006
 
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Abstract

A very simple and efficient method to prepare aminonaphthalene derivatives in good yield using the Bucherer reaction under microwave irradiation in a closed vessel is described. A reaction time of 30min at 150 Watts of microwave power was established as the optimum irradiation conditions when approximately 2 g of the initial hydroxynaphthalene was used in the synthesis.

ACKNOWLEDGMENTS

The facilities provided by CEPEDEQ, Universidad de Chile are gratefully acknowledged.

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