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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 15
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Original Articles

INDIUM MEDIATED ALLYLATION OF NITRO GROUP ON NITROBENZENE DERIVATIVES IN AQUEOUS MEDIA

Kyung Ho Kang Biochemicals Research Center, Korea Institute of Science and Technology, P.O. Box 131, Cheongryang, Seoul, 130-650, S. Korea
,
Kyung Il Choi Biochemicals Research Center, Korea Institute of Science and Technology, P.O. Box 131, Cheongryang, Seoul, 130-650, S. Korea
,
Hun Yeong Koh Biochemicals Research Center, Korea Institute of Science and Technology, P.O. Box 131, Cheongryang, Seoul, 130-650, S. Korea
,
Youseung Kim Biochemicals Research Center, Korea Institute of Science and Technology, P.O. Box 131, Cheongryang, Seoul, 130-650, S. Korea
,
Bong Young Chung Department of Chemistry, Korea University, Seoul, 136-701, S. Korea
&
Yong Seo Cho Biochemicals Research Center, Korea Institute of Science and Technology, P.O. Box 131, Cheongryang, Seoul, 130-650, S. Korea
Pages 2277-2286 | Received 25 Jul 2000, Published online: 09 Nov 2006
 
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Abstract

Indium mediated allylation of nitro group was first achieved with four allyl bromides in aqueous media. Nitro- benzenes bearing 3- and/or 4-substituent(s) gave mainly N,N-diallylated (I or I′) and/or N,O-diallylated (II) products by Method A. Allylation of nitrobenzenes having 2- (and 5-) substituent(s) could be achieved only with crotyl bromide by Method B.

ACKNOWLEDGMENTS

This project was financially supported by the Korea Ministry of Science and Technology.

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