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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 20
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Original Articles

A SIMPLE AND EFFICIENT METHOD FOR THE SYNTHESIS OF NITRILE OXIDE FROM ALDOXIME USING TRICHLOROISOCYANURIC ACID

Rogério da Conceição Rodrigues Departamento de Engenharia Química, Instituto Militar de Engenharia, Rio de Janeiro, 22290-270, Brazil
&
Alcino Palermo de Aguiar Departamento de Engenharia Química, Instituto Militar de Engenharia, Rio de Janeiro, 22290-270, Brazil
Pages 3075-3080 | Received 04 Dec 2000, Published online: 16 Aug 2006
 
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Abstract

Treatment of the aldoxime derived from vanilin with trichloroisocyanuric acid in the presence of olefins as dipolarophiles caused the formation of nitrile oxides and subsequent 1,3-dipolar cycloaddition forming the corresponding isoxazoline derivatives in good yields.

ACKNOWLEDGMENT

We thanks CAPES and FAPERJ for the financial support of this work, and Dr. Edson Ferreira da Silva, Mônica Zucolotto, Dr. Elisabete Cruz and Lab. NMR of IQ/UFRJ for spectral analysis.

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