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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 20
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Original Articles

In-MEDIATED ALLYLATION OF α-KETO ESTERS WITH ALLYL HALIDES*

Phil Ho Lee Department of Chemistry, Kangwon National University, Chunchon, 200-701, S. Korea
,
Kooyeon Lee Department of Chemistry, Kangwon National University, Chunchon, 200-701, S. Korea
&
Sukbok Chang Department of Chemistry, Ewha Womans University, Seoul, 120-750, S. Korea
Pages 3189-3196 | Received 05 Sep 2000, Published online: 16 Aug 2006
 
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Abstract

The chemoselective reaction of α-keto esters with allyl halides, propargyl bromides, and allenyl bromide using indium metal afforded α-hydroxy-γ,δ-unsaturated esters in good to excellent yields under mild conditions.

*This paper is dedicated to Professor Chang Hwan Rhee on the occasion of his 60th birthday.

ACKNOWLEDGMENT

This work was supported by Korea Research Foundation Grant (KRF-99-005-D00048). The gas chromatograms were provided by GC facility, supported by Research Center for Advanced Mineral Aggregate Composite Products.

Notes

*This paper is dedicated to Professor Chang Hwan Rhee on the occasion of his 60th birthday.

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