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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 21
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Original Articles

THE NITROMETHANE INITIATOR OF THE FRIEDEL-CRAFTS NAPHTHALENE REACTION USING MICROWAVES

G. Brãtulescu Institut National Polytechnique de Toulouse, Ecole Nationale Supérieure de Chimie, Laboratoire de Catalyse, Chimie Fine et Polymères, 118 route de Narbonne, Toulouse, Cedex 4, 31077, France
,
Y. Le Bigot Institut National Polytechnique de Toulouse, Ecole Nationale Supérieure de Chimie, Laboratoire de Catalyse, Chimie Fine et Polymères, 118 route de Narbonne, Toulouse, Cedex 4, 31077, France
&
M. Delmas Institut National Polytechnique de Toulouse, Ecole Nationale Supérieure de Chimie, Laboratoire de Catalyse, Chimie Fine et Polymères, 118 route de Narbonne, Toulouse, Cedex 4, 31077, France
Pages 3309-3313 | Received 26 Dec 2000, Published online: 20 Aug 2006
 
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Abstract

The alkylation of naphthalene using halogen derivatives may be achieved under very simple conditions by the Friedel–Crafts reaction. The products are obtained by irradiation of the paste containing the reaction mixture and a small quantity of nitromethane to initiate the reaction.

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