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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 1
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Original Articles

PYRIDINIUM FLUOROCHROMATE SUPPORTED ON WET ALUMINA: A MILD CONVENIENT REAGENT FOR THE FACILE DEPROTECTION OF ALDOXIMES

Nemai C. Ganguly Department of Chemistry, University of Kalyani, Kalyani, 741235, India
,
Prithwiraj De Department of Chemistry, University of Kalyani, Kalyani, 741235, India
,
Arun K. Sukai Department of Chemistry, University of Kalyani, Kalyani, 741235, India
&
Sripada De Department of Chemistry, University of Kalyani, Kalyani, 741235, India
Pages 1-7 | Received 06 Oct 2000, Published online: 21 Aug 2006
 
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ABSTRACT

A simple mild method of oxidative deoximation based on pyridinium fluorochromate (PFC) on wet alumina support is described. This method is particularly effective for rapid deprotection of aldoximes and aliphatic ketoximes. Sterically hindered ketoximes are resistant to the reagent.

ACKNOWLEDGMENT

One of the authors (PD) is thankful to CSIR, New Delhi for a research fellowship.

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