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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 1
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Original Articles

AN EFFICIENT AND SIMPLE PROCEDURE FOR PREPARATION OF ESTERS AND ANHYDRIDES FROM ACID CHLORIDES IN THE PRESENCE OF 1,4-DIAZABICYCLO[2.2.2]OCTANE (DABCO) UNDER SOLVENT-FREE CONDITIONS

A. R. HajipourCorrespondence[email protected]
&
Gh. Mazloumi Pharmaceutical Research Laboratory, College of Chemistry, Isfahan University of Technology, Isfahan, IR, 84156, Iran
Pages 23-30 | Received 31 Oct 2000, Published online: 21 Aug 2006
 
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ABSTRACT

A manipulatively one-pot and rapid method for the synthesis of aliphatic and aromatic ester and anhydride from acid chloride and alcohol or potassium salt of carboxylic acid under solvent-free conditions is reported. The reaction has been carried out in excellent yield and short reaction time in the presence of 1,4-diazabicyclo[2.2.2]octane (DABCO) under solvent-free conditions.

ACKNOWLEDGMENTS

Financial support of this work by the Graduate School (IUT) and the research Affairs Division of Isfahan University of Technology (IUT) is acknowledged.

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