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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 1
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Original Articles

SYNTHESIS OF PHOSPHINIC ACID ANALOGUES OF GLYCYL–GLYCINE AND CRYSTAL STRUCTURE OF N-GLYCYL-AMINOMETHYL-(PHENYLPHOSPHINIC) ACID

, , , &
Pages 79-88 | Received 15 Feb 2000, Published online: 21 Aug 2006
 

ABSTRACT

Phosphinic acid analogues of Gly-Gly, NH2CH2CONHCH2-P(R)O2H (R = Me, Ph, t-Bu), were synthesised by the active ester method from free aminomethylphosphinic acids purified on cation exchange resins. The crystal and molecular structure was determined for Gly–Gly(PPh)·H2O (R = Ph). The results point to similar bond parameters as were found for Gly–Gly and its phosphonic analogue Gly–Gly(P).

ACKNOWLEDGMENT

The work was supported by the Grant Agency of the Czech Republic (No. 203/97/0256) and by a grant of the Universita Karlova (GAUK 243/1999/B, to P.V.). We also thank the Grant Agency of the Czech Republic (No. 203/99/0067, to J. Fábry) for support of access to CCDC.

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