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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 2
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Original Articles

A FACILE REDUCTION OF AZIDES TO THE CORRESPONDING AMINES WITH Sm/NiCl2·6H2O SYSTEM

Huayue Wu
,
Rener Chen Department of Chemistry, Zhejiang University at Xixi Campus, Hangzhou, 310028, P. R. China
&
Yongmin Zhang Department of Chemistry, Zhejiang University at Xixi Campus, Hangzhou, 310028, P. R. China
Pages 189-193 | Received 15 Feb 2000, Published online: 16 Aug 2006
 
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ABSTRACT>

Azides can be easily reduced to the corresponding amines with Sm/NiCl2·6H2O in excellent yields under mild and neutral conditions.

ACKNOWLEDGMENTS

We are grateful to the National Natural Science Foundation of China (Project No. 29872010), the NSF of Zhejiang Province, China, and the Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences for financial support.

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