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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 2
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Original Articles

A NOVEL SYNTHESIS OF HEXASUBSTITUTED CYCLOTRIPHOSPHAZENES

Chengfeng Ye State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P. R. China
,
Zefu Zhang State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P. R. China
&
Weimin Liu State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P. R. China
Pages 203-209 | Received 04 Dec 2000, Published online: 16 Aug 2006
 
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ABSTRACT

Hexaaryloxyphosphazenes [N3P3(O-C6H4-R)6] (R=H, CH3, OCH3, C(CH3)3, CHO, COCH3, COOR, C6H5, NO2, F, etc) were readily obtained with ca 70% isolated yield in refluxing acetonitrile in the presence of anhydrous potassium phosphate. All compounds were characterized by means of elemental analysis, 1H-NMR, 31P-NMR spectroscopy.

ACKNOWLEDGMENTS

We are grateful to the National Natural Science Foundation of China (grant No. 59825116) and Chinese Academy of Sciences for the financial support.

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