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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 6
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Original Articles

MICROWAVE ASSISTED SYNTHESIS OF α,α′-BIS(BENZYLIDENE)KETONES IN DRY MEDIAFootnote*

J. S. Yadav Organic-I Division, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
B. V. Subba Reddy Organic-I Division, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
,
A. Nagaraju Organic-I Division, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
&
J. A. R. P. Sarma Organic-I Division, Indian Institute of Chemical Technology, Hyderabad, 500 007, India
Pages 893-896 | Received 12 Apr 2001, Published online: 16 Aug 2006
 
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ABSTRACT

Aromatic aldehydes undergo cross-aldol condensation with ketones in the presence of KF-Al2O3 under microwave irradiation in solvent-free conditions to afford the corresponding α,α′-bis(benzylidene) alkanones in high yields.

*IICT Communication No. 4420.

ACKNOWLEDGMENTS

A.N. and B.V.S. thank UGC & CSIR New Delhi for award of fellowships.

Notes

*IICT Communication No. 4420.

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