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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 12
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Original Articles

SYNTHESIS OF NEW-TYPED α,β-UNSATURATED ACYL AZO COMPOUNDS WITH NaBrO3/H2SO4 AS THE OXIDATIVE SYSTEM

Yu-lu Wang Department of Chemistry, Henan Normal University, Xinxiang, Henan, 453002, P.R. China; The Key Laboratory of Environmental Science and Technology of High Education of Henan Province, Henan, P.R. ChinaCorrespondence[email protected]
,
Yue-wei Zhao Department of Chemistry, Henan Normal University, Xinxiang, Henan, 453002, P.R. China; The Key Laboratory of Environmental Science and Technology of High Education of Henan Province, Henan, P.R. China
,
Xiao-xia Wang Department of Chemistry, Henan Normal University, Xinxiang, Henan, 453002, P.R. China; The Key Laboratory of Environmental Science and Technology of High Education of Henan Province, Henan, P.R. China
&
Zhi-fang Duan Department of Chemistry, Henan Normal University, Xinxiang, Henan, 453002, P.R. China; The Key Laboratory of Environmental Science and Technology of High Education of Henan Province, Henan, P.R. China
Pages 1781-1785 | Received 02 Aug 2000, Published online: 17 Oct 2011
 
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ABSTRACT

Eight new-typed α,β-unsaturated acyl azo compounds were prepared for the first time using NaBrO3/H2SO4 as the oxidant with simple stirring apparatus at room temperature. NaBrO3 was first reported as an efficient dehydrogenating agent in this paper.

Acknowledgments

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