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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 12
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Original Articles

A FACILE METHOD FOR THE SYNTHESIS OF BENZOTHIACROWN ETHER FORMYL DERIVATIVES

Olga A. Fedorova Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
,
Artem I. Vedernikov Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
,
Olga V. Yescheulova Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
,
Yulia V. Pershina Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
,
Pavel V. Tsapenko Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
&
Sergey P. Gromov Photochemistry Center of the Russian Academy of Sciences, Novatorov str., 7a, Moscow, 117421, Russia
Pages 1909-1915 | Received 27 Jun 2001, Published online: 17 Oct 2011
 
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ABSTRACT

A facile route to the formyl derivatives of benzothiacrown ethers with different combinations of O and S heteroatoms in the macrocycle involving ring closure reactions of substituted benzaldehydes with dithiols was developed. The effects of alkali metal cations and solvent were studied.

ACKNOWLEDGMENT

The study was supported by the INTAS (96-1142), DFG (Grant 436RUS 113/56/0), RFBR-DFG (Grant 98-03-04137) and the Ministry for Science and Technologies of Russia.

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