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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 32, 2002 - Issue 13
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Original Articles

DEIODINATION OF IODOLACTONES BY TRANSFER HYDROGENOLYSIS USING RANEY NICKEL AND 2-PROPANOL

Robert C. Mebane Department of Chemistry, University of Tennessee at Chattanooga, Chattanooga, TN, 37403-2598, U.S.A.Correspondence[email protected]
,
Kimberly D. Grimes Department of Chemistry, University of Tennessee at Chattanooga, Chattanooga, TN, 37403-2598, U.S.A.
,
Summer R. Jenkins Department of Chemistry, University of Tennessee at Chattanooga, Chattanooga, TN, 37403-2598, U.S.A.
,
Jonathan D. Deardorff Department of Chemistry, University of Tennessee at Chattanooga, Chattanooga, TN, 37403-2598, U.S.A.
&
Benjamin H. Gross Department of Chemistry, University of Tennessee at Chattanooga, Chattanooga, TN, 37403-2598, U.S.A.
Pages 2049-2054 | Received 24 Jul 2001, Published online: 16 Aug 2006
 
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ABSTRACT

Raney nickel in refluxing 2-propanol is an effective catalytic system for reducing iodolactones into their corresponding lactones.

ACKNOWLEDGMENTS

The authors gratefully acknowledge financial support from the University of Chattanooga Foundation and the Grote Chemistry Fund. In addition, we are indebted to the W.R. Grace Company, Chattanooga for the generous donation of Raney nickel catalyst.

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